TiCx with different morphologies were synthesized from combustion synthesis of Ni–Ti–C system by changing the reactant C/Ti ratio. High stoichiometry of TiCx changed the growth direction from (111) to (100) surface and therefore resulted in cubic morphology while high combustion temperature at high reactant C/Ti ratio led to the roughening transition of (100) surface and form spherical morphology.
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Yang et al. (2012) studied this question.
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