Abstract [2H6]‐3‐Mercapto‐3‐methylbutyl formate was synthesized to be used as internal standard in the quantification of the corresponding unlabelled thiol which belongs to the character impact flavour compounds of roasted coffee. 1H‐NMR, 13C‐NMR and mass spectra are given and compared with those of the unlabelled thiol.
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Masanetz et al. (1995) studied this question.
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