Facile synthesis of 2‐n‐dodecylthio‐4‐phenylthiomethyl‐1,3,4‐thiadiazole‐5‐thione 6, starting from 2,5‐dimercapthothiadiazole via 2‐n‐dodecylthio‐1,3,4‐thiadiazole‐5‐thione 2, 2‐n‐dodecylthio‐4‐hydroxymethyl‐1,3,4‐thiadiazole‐5‐thione 4 and 2‐n‐dodecylthio‐4‐chloromethyl‐1,3,4‐thiadiazole‐5‐thione 5 is described.
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Katritzky et al. (1990) studied this question.