Fourier transform infrared (FTIR) spectroscopy with transmission cell is described to predict anisidine value of palm olein. The calibration set was prepared by mixing the thermally oxidized palm olein and the unoxidized palm olein with certain ratios (w/w) covering a wide range of anisidine values. A partial least square (PLS) regression technique was employed to construct a calibration model. This model was further accomplished by a validation step. The standard error of prediction found was 0.51. The precision of this method was shown to be comparable to the accuracy of the American Oil Chemists’ Society method used for measurement of anisidine value, with coefficient of determination (R2) of 0.99. The study showed that mid‐band FTIR spectroscopy combined with a PLS calibration technique is a versatile, efficient, and accurate technique for the estimation of anisidine value of palm olein within about 2 min with less than 2 mL of sample.
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Man et al. (1999) studied this question.
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