We propose a method derived from fast Fourier transform (FFT) process to measure the characteristic length scale of bicontinuous nanoporous structures. By rotationally averaging the FFT power spectrum of a nanoporous micrograph from scanning electron microscope (SEM) or transmission electron microscope (TEM), a significant peak in the power spectrum can be obtained, which reflects the characteristic length scale of the quasi-periodic structure. This method is demonstrated for the bicontinuous morphology that is frequently observed in nanoporous metals prepared by chemical or electrochemical dealloying.
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Fujita et al. (2008) studied this question.
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