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Urea/n‐paraffin clathrates enable Raman spectroscopic studies of oriented single n‐paraffin molecules in the extended planar zig‐zag configuration to be made. Raman spectra in the region 0–3500 cm−1 are reported for various orientations of single crystals of the following urea and urea‐d4/n‐paraffin clathrates: urea/n‐tetradecane, urea/n‐hexadecane and urea/n‐undecane. Assignments have been made for the vibration of the urea host lattice and the guest n‐paraffin molecules in the extended planar zig‐zag configuration, utilising the orientation measurements.
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Fawcett et al. (1975) studied this question.
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