Bis(L-α-glyceryl) phosphoric acid has been prepared by synthesis. It was obtained by phosphorylating D-acetone glycerol with phenylphosphoryl dichloride in the presence of pyridine, and freeing the intermediate product, bis(acetone L-α-glyceryl) phosphoric acid phenyl ester, of its protective groups by catalytic hydrogenolysis and mild acid hydrolysis.
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Baer et al. (1958) studied this question.
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