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September 15, 2026Journal of Natural FibersOpen Access

Structure–Property Relationships in Alkali-Treated Pineapple Leaf Fiber Reinforced PLA Composites: Influence of Fiber Loading and Processing-Induced Effects

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Authors

RDRajeevan Sheela DarsanBRB. Stanly Jones RetnamSSS.M. Sapuan

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Overview

Experimental study demonstrates processing-induced defects reduce tensile strength in alkali-treated pineapple fiber PLA composites, highlighting critical manufacturing trade-offs.

Key Points

  • To assess the influence of alkali surface treatment, fiber loading, and melt-processing phenomena on the microstructure and mechanical properties of pineapple leaf fiber-reinforced PLA composites.
  • Compounded untreated (UPF) and alkali-treated pineapple leaf fibers (APF) into polylactic acid (PLA) at 5–20 wt.% loadings using twin-screw melt blending followed by injection molding.
  • Characterized composite properties using differential scanning calorimetry (DSC), dynamic mechanical analysis (DMA), tensile testing, void content analysis, water absorption testing, and fracture morphology.
  • Alkali treatment decreased the average fiber diameter from 138.8 μm to 92.2 μm, while fiber incorporation promoted heterogeneous nucleation with glass transition temperatures between 54–59 °C.
  • Tensile modulus increased by more than 45%, and the 10 wt.% untreated fiber composite achieved the highest storage modulus.
  • Tensile and flexural strengths declined at higher fiber loadings and in multiple treated composites due to increased void content, porosity, fiber pull-out, and processing-induced fiber damage.

Cite This Study

Darsan et al. (2026) studied this question.

synapsesocial.com/papers/6aa9132f9013453be30a0eeehttps://doi.org/10.1080/15440478.2026.2726705
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