Carbon atom correlations become interesting in 3D NMR spectroscopy if one selects CH2 groups with an inverse DEPT sequence in such a way that the spectral breadth in two of the dimensions is limited. 3 D DEPT‐TOCSY has made it possible to obtain, within about ten hours and with a very good signal‐to‐noise ratio, a high‐resolution 13C‐resolved 3D NMR spectrum of a cyclic hexapeptide.
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Schmieder et al. (1990) studied this question.
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