The first stable molecular Fev complex, [Fev(I)(′N2S2′)], forms in the metal-centered oxidation of the readily accessible FeIV complex [FeIV(pnPr3)(′N2S2′)] with elemental iodine according to Equation (a). The high-valent character of the iron center is proved by structural, spectroscopic, and electrochemical data.
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Sellmann et al. (1997) studied this question.
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