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A new general synthesis method for hypervalent diorganoantimony( iii ) fluorides with pendant arm ligands is based on treatment with [Bu 4 N]F·3H 2 O of cationic species e.g. [{2-(2′,6′- i Pr 2 C 6 H 3 NCH)C 6 H 4 } 2 Sb] + [PF 6 ] − or [{2-(Me 2 NCH 2 )C 6 H 4 }PhSb] + [SbF 6 ] − .
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Preda et al. (2015) studied this question.
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