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(opens in new window) Buy Article (opens in new window) Permissions and Reprints (opens in new window) All articles of this category (opens in new window) Stereoselective construction of 3-trifluoromethyl conjugated dienoates or enynoates was achieved from ethyl ( Z )-4,4,4-trifluoro-3-iodobutenoate and alkenyltin or alkynyltin reagents through the Stille reaction. Reduction of ethyl 3-trifluoromethyldienoates using DIBAL-H selectively afforded allylic alcohols. conjugated 3-trifluoromethyl dienoates or dienols - Stille cross-coupling reaction - vinyltin reagents - vinylic iodide - substitution - reduction
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Prié et al. (1998) studied this question.
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