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December 14, 2005Journal of the American Ceramic Society

Neck Formation and Self‐Adjusting Mechanism of Neck Growth of Conducting Powders in Spark Plasma Sintering

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Authors

XSXiaoyan SongQingdao UniversityXLXuemei LiuTongji UniversityJZJiuxing ZhangHefei University of Technology

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Implication

Experimental study reveals a self-adjusting neck growth mechanism during spark plasma sintering of copper powders, indicating how pulsed current drives uniform microstructure formation.

Key Points

  • To elucidate the mechanisms controlling neck formation and neck growth in conducting spherical copper powders under pulsed direct current during spark plasma sintering.
  • Examined the microstructures of spherical copper powder particles across distinct stages of the spark plasma sintering process.
  • Developed theoretical models to quantify the local temperature distributions and electrical current intensity effects across particle-contact interfaces.
  • Pulsed direct current created severe temperature gradients between particle surfaces and centers, reaching the material's boiling point at contact surfaces to initiate neck formation through local melting and rapid solidification.
  • Neck growth was governed by a dynamic competition between widening neck cross-sectional area and rising temperature-dependent electrical resistivity.
  • Identified a self-adjusting coarsening mechanism that naturally homogenizes neck dimensions and fine-grain sizes throughout the neck zones.

Cite This Study

Song et al. (2005) studied this question.

synapsesocial.com/papers/6aae36fac763f45372cc6645https://doi.org/10.1111/j.1551-2916.2005.00777.x
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