A novel reported method for preparation of the first thiophene thioglycosides via a one-pot reaction of sodium thiophenethiolate salts with 2,3,4,6-tetra-O-acetyl-α-D-gluco- and galactopyranosyl bromides has been studied. The sodium thiophenethiolate salts were prepared using sodium cyanoethylene thiolate salts.
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Elgemeie et al. (2009) studied this question.
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