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A new type of chemically modified electrode, named Mo-S-Ag cluster modified electrode, was prepared by adsorption of MoS42– on the surface of a silver electrode. The modified electrode was characterized by spectroscopic methods, including FT-IR, FT-Raman, XPS and AES. The experimental results indicated that MoS42– was bound to the surface of a silver electrode, forming Mo-S-Ag ‘bridges’. The modified electrode possessed a strong electrocatalytic activity towards the oxidation of ascorbic acid (AA). Differential pulse voltammetric response (DPV) at the modified electrode also showed good results.
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Zhu et al. (1998) studied this question.
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