Dedicated to the member of Russian Academy of Sciences, Professor Aslan Tsivadze on the occasion of his Anniversary The symmetrically substituted hexakis(n-hexyl)hemihexaphyrazine was synthesized by condensation of 3,6-bis(n-hexyl)phthalonitrile and 2,5-diamino-1,3,4-thiadiazole in the presence of sodium pentanolate. The macrocycle was characterized by MALDI-TOF mass spectrometry, as well as IR, 1H and 13C NMR, UV-Vis absorption and fluorescence spectroscopies.
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Kibireva et al. (2023) studied this question.
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