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Single-crystal X-ray diffraction analysis of PdCl2(dppfO2) [dppfO2 = 1,1′-bis(oxodiphenylphosphoranyl)ferrocene] shows a rare tetrahedral geometry at a d8 metal centre; physical and spectroscopic characterisations indicate a paramagnetic species.
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Yeo et al. (1999) studied this question.
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