Taking the tube: A silica-supported palladium catalyst packed into teflon tubing is a simple, low-cost, and effective method for carrying out carbonylative cross-coupling reactions of arylhalides with amines and radiolabeled carbon monoxide gas. In carbonylation reactions, the microtube reactor displays enhanced yields over a short time period (12 min) compared with batch methods.
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Miller et al. (2007) studied this question.
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