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Thiazyl Pentafluorooxotellurate, NSOTeF5 The title compound 3 is prepared from NSF and B(OTeF5)3 or from NS+SbF6− and CsOTeF5, respectively. 3 is rather unstable and isomerises rapidly to give the known TeF5NSO (2) and polymeric products. F5TeNSNTeF5 (4) is formed from 2 in the BF3‐ catalyzed elimination of SO2. From 3 and AsF5 the thiazyl salt NS+F5TeOAsF5− (6) is formed.
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Hoppenheit et al. (1985) studied this question.
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