Trimethylsilyl azide (TMSN 3 ) as a cheap and easily available azide/amine source is showing increasingly important applications in photocatalytic and electrochemical organic synthesis. This mini‐review systematically summarizes the latest applications of TMSN 3 in photocatalytic and electrocatalytic organic synthesis, and discusses the related mechanisms and development prospects.
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Ji et al. (2026) studied this question.
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