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A tandem azide-alkyne cycloaddition (CuAAC)/C-C coupling strategy enabled the efficient construction of bitriazole scaffolds from calcium carbide. Subsequent energetic functionalization afforded two new nitrogen-rich energetic derivatives, including a novel trinitromethyl-substituted compound. This work expands the synthetic utility of tandem CuAAC/C-C coupling chemistry and demonstrates the potential of calcium carbide-derived bitriazole scaffolds as versatile building blocks for energetic materials.
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Cheng et al. (2026) studied this question.
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