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September 29, 2025NanofabricationOpen Access

Green Approach to Beckmann Rearrangement of Cyclohexanone Oxime Using Nanostructured ZSM-5 Zeolite

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Authors

LRL. Selva RoselinRSR. SavidhaKAKhadijah H. Alharbi

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Overview

This approach demonstrates efficient conversion of cyclohexanone oxime into ε-caprolactam using zsm-5 catalysts, highlighting green chemistry benefits.

Key Points

  • ZSM-5 nanoparticles achieved the highest conversion of cyclohexanone oxime, resulting in effective ε-caprolactam synthesis.
  • Under optimized conditions, a catalyst loading of 0.10 g and a reaction temperature of 120°C were pivotal for efficiency.
  • Catalysts exhibited easy recovery and recyclability, which supports sustainable and green chemistry principles.
  • Characterization techniques included DLS, XRD, FT-IR, N2 adsorption–desorption isotherms, and NMR analysis, ensuring thorough assessment.

Cite This Study

Roselin et al. (2025) studied this question.

synapsesocial.com/papers/68da58d1c1728099cfd10e41https://doi.org/10.37819/nanofab.10.2079
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Also Consider

Synapse has enriched 5 closely related papers on similar clinical questions. Consider them for comparative context:

  1. 1Synergistic Effect of Hierarchical ZSM‐5 Zeolites Promotes Synthesis of Bioderived 4‐Hydroxy‐2‐Cyclopentenones and p‐Xylene2025
  2. 2In situ Generation of Cyclohexanone Drives Electrocatalytic Upgrading of Phenol to Nylon‐6 Precursor2024 · 37 citations
  3. 3In situ Generation of Cyclohexanone Drives Electrocatalytic Upgrading of Phenol to Nylon‐6 Precursor2024
  4. 4Integrated process design and safety analysis for caprolactam production via the cyclohexanone route: Oxime reactor balancing, beckmann rearrangement, and packed bed reactor mechanical engineering2026
  5. 5Zeolites as efficient catalysts for synthesis of cyclopentyl ethyl ether2025