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This method demonstrates alkylarylation in alkenes and alkynes under photoredox conditions, suggesting broad functional group tolerance.
Herein, we report a strategy for the alkylarylation of unsaturated carbon-carbon bonds, wherein bis(sulfones) serve as dual-source donors to deliver alkyl and aryl groups in a single step, redefining their reactivity paradigm. Both alkenes and alkynes undergo efficient difunctionalization with broad functional group tolerance. Mechanistic studies reveal a cascade involving deprotonation, single-electron oxidation, radical addition and Smiles rearrangement.
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Wang et al. (2025) studied this question.
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