Chemically Stable NiMoO₄/NRGO Asymmetric Capacitor

In this work, a chemically stable NiMoO 4 /NRGO nanocomposite was prepared via a facile hydrothermal method. The flower‐like structure of NiMoO 4 (NMO) nanoparticles is randomly distributed on the surface of nitrogen‐doped reduced graphene oxide (NRGO) sheets, as observed in FESEM images. Compared to related reports, the NMO/NRGO (II) nanocomposite exhibits an excellent high surface area of 368.9 m 2 g −1 and a mesoporous nature, as shown in N₂ adsorption‐desorption isotherms. The specific capacitance of the NMO/NRGO (II) electrode is 721 F g −1 at 1 A g −1 using a 6 M KOH electrolyte, retaining 91.2 % of its initial value after 5000 cycles. Electrochemical impedance spectroscopy (EIS) reveals that the electrode has a lower charge‐transfer resistance, indicative of good electrochemical behavior. An asymmetric device consisting of NMO/NRGO (II) || activated carbon (AC) electrodes exhibits a high energy density of 49.1 Wh kg −1 at 524.4 W kg −1 within a voltage range of 1.4 V, retaining 89 % of its initial capacitance after 5000 cycles, demonstrating good cyclic durability. These results suggest that the NMO/NRGO (II) electrode is a promising active material for supercapacitor devices.