Synthesis of protected precursors of cyclic β-1,6-oligoglucosamines by electrochemical polyglycosylation of thioglycosides as a monomer is performed. The monomer with 2,3-oxazolidinone protecting group afforded the cyclic disaccharide exclusively. Cyclic oligosaccharides up to trisaccharide were obtained using the monomer with 2-deoxy-2-azido group.
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Rahman et al. (2024) studied this question.
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