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This research demonstrates controlled C–H cyanation and thiocyanation in indolizines, implying key roles of NH4SCN and H2O2.
An efficient and controlled approach for C–H cyanation/thiocyanation of indolizines is reported under visible‐light‐induced conditions. NH 4 SCN is used as the cyano or thiocyano source and the presence or absence of H 2 O 2 are found to be the key factor in the selective construction of C‐3 cyano or thiocyano indolizines. A set of control experiments, such as radical trapping experiments and fluorescence quenching studies are conducted to assess mechanistic insights of the reaction.
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Jiang et al. (2025) studied this question.
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