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January 14, 2026Materials2 citationsOpen Access

Effect of In Situ Synthesized Al2O3 and TiC on the Microstructure and Properties of 6061 Aluminum Matrix Composites

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WLWei LongJZJiaxin ZhouXHXinbin Hu

Key Points

  • This research aims to investigate how in situ synthesized Al2O3 and TiC affect the properties of 6061 aluminum matrix composites.
  • Fabricated Al2O3-TiC/6061Al composites via in situ powder metallurgy.
  • Studied effects of sintering temperature and ceramic content on microstructure.
  • Measured mechanical properties like tensile strength and microhardness.
  • Analyzed wear performance under different loads.
  • At 1000 °C and 1100 °C, the microstructure included Al3Ti, Al2O3, and TiC phases.
  • At 1200 °C, the microstructure predominantly featured Al2O3 and TiC.
  • The composite at 1200 °C had a tensile strength of 246 MPa and microhardness of 104.2 HV0.1.
  • Under a 30 N load, the composite exhibited the lowest friction coefficient (0.253) and wear rate (0.396 mm3·N−1·m−1).
  • Dominant wear mechanism shifted from delamination for aluminum alloy to abrasive wear for the composite.

Abstract

Al2O3-TiC/6061Al composites were fabricated via in situ powder metallurgy using 6061 Al, TiO2, and graphite powders as starting materials. The effects of sintering temperature and ceramic particle content on the microstructure and mechanical properties of the composites were investigated. The wear performance of composites sintered at 1200 °C with varying ceramic particle content was also examined. The results indicate that the microstructure of the composite varied with the sintering temperature. At 1000 °C and 1100 °C, the microstructure primarily consisted of Al3Ti, Al2O3, and TiC phases. At 1200 °C and 1250 °C, the microstructure was predominantly composed of Al2O3 and TiC phases. The 6061 Al-12% (TiO2 + C) composite sintered at 1200 °C exhibited a tensile strength of 246 MPa, an elongation of 12.7%, and a microhardness of 104.2 HV0.1. Regarding wear performance, the wear behavior of the composites under different loads at 1200 °C was studied. Under a 30 N load, the 6061 Al-12% (TiO2 + C) composite demonstrated the lowest friction coefficient and wear rate, measured at 0.253 and 0.396 mm3·N−1·m−1, respectively. Analysis of the worn surface morphology under a 30 N load indicates that the dominant wear mechanism for the 6061 aluminum alloy is delamination wear, whereas for the 6061 Al-12% (TiO2 + C) composite, it is primarily abrasive wear.

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Cite This Study

Long et al. (2026) studied this question.

synapsesocial.com/papers/696719c1c0d1e3cfbfce92dbhttps://doi.org/10.3390/ma19020308
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