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This research reveals a method for synthesizing perfluoroalkylated benzazepines and benzoxepines using visible light, suggesting a greener approach to complex organic synthesis.
A visible-light-mediated perfluoroalkylation/cyclization of N-allyl-N-(2-(3,3-bis(methylthio)acryloyl)aryl)-4-methylbenzenesulfonamides and 1-(2-(allyloxy)aryl)-3,3-bis(methylthio)prop-2-en-1-ones for the synthesis of perfluoroalkylated benzazepines and benzoxepines is developed. This protocol features photocatalystfree, simple operation, and good regioselectivity, providing a novel environmentally...
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Pan et al. (2026) studied this question.
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