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Dataset presents powder particle distribution across mechanochemical synthesis times, implying potential for improved thermoelectric materials.
This data is additional material to the article "Optimisation of the time mechanochemical synthesis of thermoelectric material Mg3Sb2-Mg3Bi2" in RSC Mechanocemistry. This file presents only a partial work, due to the limited number of uploadable files. The first part of the work consists of creating a dataset of initial SEM images in BSE mode for subsequent processing for powders after 1, 3, 5, 7, and 9 hours of mechanochemical synthesis (9 photos each). The second part consists of segmented images of powders after 1, 3, 5, 7, and 9 hours of mechanochemical synthesis (9 powders each) using image processing. The third part consists of constructed histograms of the particle size distributions of powders after 1, 3, 5, 7, and 9 hours of mechanochemical synthesis.
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Mikhailova et al. (2026) studied this question.
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