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March 27, 2026Journal of Chemical & Engineering Data4 citations

Revisiting the Definition, Solid–Liquid Equilibria, and Thermodynamic Nonideality of Deep Eutectic Solvents

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SMShaibuna MachingalRGRamesh L. Gardas

Key Points

  • To clarify the definition and thermodynamic behaviors of deep eutectic solvents (DESs) for better application.
  • Reviewed definitions and properties of DESs
  • Examined phase behavior and thermodynamic nonideality
  • Outlined solid-liquid equilibrium phase diagram construction
  • Summarized recent studies on SLE determination of DESs
  • Provided a clear thermodynamically grounded definition for DESs
  • Outlined essential components needed for DES formation
  • Highlighted the critical role of phase diagrams in defining DESs
  • Discussed the impact of water on DES stability and future research directions

Abstract

Since their introduction, deep eutectic solvents (DESs) have been widely used, often without a rigorous or consistent definition. This has led to misuse of the term, where DESs are applied without considering their underlying thermodynamics, resulting in misclassification and studies that overlook essential physicochemical behaviors. This review aims to provide a comprehensive understanding of DESs by examining their definitions, thermodynamic properties, phase behavior, and modeling approaches through representative examples. First, common misconceptions regarding DES definitions are addressed, followed by a clear, thermodynamically grounded definition. Next, the types of components capable of providing the nonideal thermodynamic interactions necessary for DES formation are outlined. The review then emphasizes the importance of constructing solid–liquid equilibrium (SLE) phase diagrams for accurately defining DESs, discussing both experimental and thermodynamic modeling methods for determining these diagrams. Recent studies on SLE determination of DESs using various approaches are also summarized. Finally, the effects of water on DES stability and other challenges are discussed, along with perspectives for future research. Overall, DES research holds great promise, and this review supports the rational design, selection, and modeling of DESs, which are essential for efficient and practical process development.

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Cite This Study

Machingal et al. (2026) studied this question.

synapsesocial.com/papers/69c6201515a0a509bde187f7https://doi.org/10.1021/acs.jced.5c00781
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