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Advanced organic synthesis demonstrates efficient synthesis of glucopyranose pentaacetates, suggesting a safe method for students.
An advanced-level organic synthesis experiment is described. The experiment accomplishes the synthesis of α-and β-D-(+)-glucopyranose pentaacetates in a convenient and safe manner, avoiding the use of zinc chloride and fused sodium acetate. Students isolate the pure acetates in a regular laboratory period and identify them by melting points and their characteristic NMR spectra.
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Pandita et al. (2007) studied this question.
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