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April 4, 2026JACOW0 citationsOpen Access

First steps into the operation of the SAPOTI cryogenic nanoprobe at the CARNAÚBA beamline at Sirius/LNLS

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VFVinícius Bomfim FalchettoASAnna Paula da Silva SoteroANAntônio Carlos Piccino Neto

Key Points

  • The research aims to demonstrate the operational capabilities of the SAPOTI cryogenic nanoprobe and its integration at the CARNAÚBA beamline.
  • Utilized multi-analytical x-ray techniques including absorption, diffraction, and spectroscopy.
  • Developed a high-performance cryogenic sample stage for single-nanometer imaging.
  • Commissioned the system by performing KB alignment and assessing focus stability.
  • Achieved highly stable beam sizes between 30 to 120 nm.
  • Established monochromatic flux of up to 1e11 photons per second.
  • Demonstrated potential for advanced imaging techniques like ptychography and absorption imaging.

Abstract

SAPOTI is the second nanoprobe at the CARNAÚBA (Coherent X-Ray Nanoprobe Beamline) beamline at the 4th-generation light source Sirius/LNLS. Working from 2.05 to 15 keV, it relies on simultaneous multi-analytical X-ray techniques (absorption, diffraction, spectroscopy, fluorescence and luminescence) and imaging in 2D and 3D. It has been designed for highly-stable fully-coherent beam sizes from 30 to 120nm, and monochromatic flux up to 1e11ph/s/100mA/0.01%BW after an achromatic KB (Kirkpatrick-Baez) focusing optics. Moreover, a new in-vacuum high-performance cryogenic sample stage has been developed aiming at single-nanometer resolution images. The nanoprobe is now successfully installed and technical commissioning is underway. The focus of this work is two-fold. Firstly, it highlights the system integration results at the beamline, namely: overall thermo-mechanical performance of the KB mirrors and sample stage. And, finally, it showcases the instrument’s technical commissioning results, namely: KB alignment and focus stability, and initial fly-scan potential for ptychography and absorption imaging.

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Cite This Study

Falchetto et al. (2026) studied this question.

synapsesocial.com/papers/69d0ae94659487ece0fa47d1https://doi.org/10.18429/jacow-medsi2025-tuob03
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