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November 26, 2024Metallurgical and Materials Transactions AOpen Access

Microstructure Development in Duplex Stainless Steels from Additive Manufacturing with Coaxial Directed Energy Deposition and Heat Treatment

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Authors

THTrond Arne HasselLMLene Anita MarkenSASiri Marthe Arbo

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Overview

Experimental study demonstrates improved toughness and phase balance in additively manufactured duplex stainless steels after solution annealing, highlighting pathways to eliminate brittle phases.

Key Points

  • To investigate the microstructural evolution and mechanical performance of additively manufactured duplex stainless steel grades 2205, 2209, and 2509 during solution annealing.
  • Fabricated specimens from duplex stainless steel grades 2205, 2209, and 2509 using wire-fed coaxial directed energy deposition.
  • Conducted post-build solution annealing at temperatures between 1020 and 1170 °C and compared microstructures with thermodynamic equilibrium calculations.
  • Evaluated phase morphology, hardness, and Charpy impact toughness on as-built and heat-treated grade 2209 samples.
  • Grades 2209 and 2509 achieved more homogeneous microstructures with higher austenite fractions as-built than 2205, but required higher annealing temperatures than conventional duplex alloys to suppress sigma phase precipitation.
  • Post-deposition heat treatment significantly enhanced the Charpy impact toughness of grade 2209 compared to its as-built condition.
  • Optimized heat treatment prevented detrimental phase precipitation while maintaining controlled grain growth and yielding a fine-grained, slightly spheroidized Widmanstätten austenite morphology.

Cite This Study

Hassel et al. (2024) studied this question.

synapsesocial.com/papers/69d8fd5ea5ecc596b5d18f80https://doi.org/10.1007/s11661-024-07560-z
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