A new MAS NMR probe for in situ investigations of hydrocarbon conversion on solid catalysts under continuous-flow conditions

Michael Hunger; Thomas D. Horvath

doi:10.1039/c39950001423

January 1, 1995Journal of the Chemical Society Chemical Communications

A new MAS NMR probe for in situ investigations of hydrocarbon conversion on solid catalysts under continuous-flow conditions

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Key Points

To develop and demonstrate an in situ magic angle spinning (MAS) NMR probe capable of monitoring hydrocarbon conversion on solid catalysts under continuous-flow reaction conditions.
Designed a specialized MAS NMR probe configuration equipped to deliver continuous reactant fluid flow directly to the catalyst sample.
Conducted in situ NMR measurements of catalytic hydrocarbon conversions occurring on solid catalyst surfaces under steady-state continuous-flow conditions.
Successfully performed in situ MAS NMR spectroscopy during active continuous-flow hydrocarbon reactions on solid catalysts.
Enabled the real-time detection and characterization of catalytic reaction steps and surface-bound intermediates under operational flow conditions.

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Implication

Experimental study demonstrates a continuous-flow magic angle spinning NMR probe for solid catalysts, enabling real-time monitoring of hydrocarbon conversion.

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Hunger et al. (1995) studied this question.

synapsesocial.com/papers/69dac8427a67537a8ba3c7f7 https://doi.org/10.1039/c39950001423

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A new MAS NMR probe for in situ investigations of hydrocarbon conversion on solid catalysts under continuous-flow conditions

Key Points

No abstract yet

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Implication

Discussion

Cite This Study

A new MAS NMR probe for in situ investigations of hydrocarbon conversion on solid catalysts under continuous-flow conditions

Key Points

No abstract yet

Ask about this paper

Implication

Discussion

Cite This Study

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