Synthesis of diastereomeric ligands reveals improved NMR probing capabilities in coordination chemistry.
Two diastereomeric P , P *-phosphine-diamidophosphites featuring a 1,3,2-diazaphospholidine ring and an oxalamide scaffold were synthesized. These C 1 -symmetric ligands are far more convenient for probing coordination by NMR than C 2 -symmetric bisdiamidophosphite or bisphosphine...
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Chuchelkin et al. (2026) studied this question.
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