Demonstrates an efficient method for disulfenylation of anilines, highlighting green chemistry benefits.
We report herein a green, efficient electrochemical oxidation protocol for the disulfenylation of anilines, which enables bis(C-S) bond construction without transition metal catalysts or external oxidants and affords the desired bis-sulfenylated aniline derivatives in yields up to 73% with broad aryl/alkyl thiol compatibility.
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Chen et al. (2026) studied this question.
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