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Wheelin' and dealin': The M10 molecular wheels M10(OMe)20(O2CR)10 (M=Ga, R=Me; M=Fe, R=Ph) were modified to M18 wheels in a nontemplate synthesis upon incorporation of a diolate ligand (see space-filling model of Ga18(pd)12(pdH)12(O2CMe)6(NO3)66+; Ga yellow, O red, N blue, C gray; pdH2=1,3-propanediol). Remarkably, dissolution in MeOH converts both M18 wheels back into the M10 wheels.
King et al. (Wed,) studied this question.
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