The crystal structure of bis(m 2 -2-((dimethylamino)methyl)-6-ethoxyphenolato-k 3 O:O,N)-bis(m 2 -2-((dimethylamino)methyl)-6-ethoxyphenolato-k 3 O,O′,N) bis(m 2 -azido-k 2 N:N)-bis(azido-k 1 N)tetracobalt(II), C 44 H 64 Co 4 N 16 O 8

Key Points

• To determine the crystal structure of a novel tetracobalt(II) complex with azido and phenolato ligands.
• Determined crystal structure using X-ray diffraction techniques.
• Characterized compound C44H64Co4N16O8 in a triclinic unit cell.
• Crystal parameters: a = 10.6866 Å, b = 11.5525 Å, c = 12.0882 Å, V = 1287.3(2) Å3.
• Space group P1 with Z = 1.
• Refinement yields Rgt(F) = 0.043, wRref(F2) = 0.108.