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Novel triphenylphosphine-mediated reaction demonstrates high yields of indeno[1,2-b]oxepins, suggesting new synthetic routes.
A novel unprecedented triphenylphosphine-mediated [4 + 3] annulation reaction of 2-benzylidene indane-1,3-diones and -diynoates through initial phosphine α-addition was discovered and found to result in biologically interesting indeno[1,2-b]oxepin-4-ylidenes in up to 75% yield. The seven-membered separable Z and E isomeric oxepins were confirmed using single-crystal X-ray diffraction.
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Nallapati et al. (2022) studied this question.
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