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D‐(+)‐xylose has been converted to (+)‐sesbanimide A in sixteen steps. The synthetic scheme involves an unusual tricyclic silylated derivative ( 9a ) of the monobenzoylated product of the earlier described glutarimide intermediate ( 7 ). Compound 9a is a pivotal intermediate for the construction of ring C of (+)‐sesbanimide A.
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Vloon et al. (1991) studied this question.
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