Sugars were separated gas chromatographically on short apolar glass capillary columns by using cold, on‐column injection (OCI) techniques. After silylation, oligomers up to the hexasaccharides could be efficiently separated in resonable retention times. Response factors of silylated sugars were determined as a function of varying sample amounts and concentrations. The optimum injection amount was found to be 1 μl in heptane as solvent.
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Traitler et al. (1984) studied this question.
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