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2- O -Benzylglycerol was treated with 1,2- O -isopropylidene-L-glycerol 3-dihydrogen phosphate and dicyclohexylcarbodi-imide in dry pyridine. Deacetonation and ion-exchange chromatography of the reaction products yielded the 2- O -benzyl ether of 1,3-di- O -(glycerol-3'-phosphoryl)glycerol, from which the benzyl group was removed by catalytic hydrogenation.
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P. Plackett (1964) studied this question.
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