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Synthetic mullite prepared from clay alumina mixture was sintered around 1400°C and at 1600°C to obtain controlled porosity. The sintered compacts were subjected to thermal shock between 1400°C and room temperature, and mechanical strength was evaluated by compressive test measurements at room temperature.The porous (∼20% OP) samples showed densification during thermal shocks. The compressive strength increased up to five thermal cycles and decreased thereafter. The least porous (0.5 to 6% OP) samples retained the strength during thermal shocks while impervious (<0.5% OP) samples showed steady increase in strength. The samples sintered at 1600°C, though impervious, had low strength and cracked after five thermal cycles due to the separation of glassy phase from the matrix resulting in conchoidal fracture.
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Dalvi et al. (1992) studied this question.
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