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Nanocrystalline TiN powder has been synthesized by the direct nitridation of nanocrystalline TiO 2 powder. Powder XRD patterns indicated that the TiN nanocrystalline powder could be obtained by nitridation at 800°C for 5 h. TEM micrographs showed that the synthesized TiN powders consisted of uniform spherical particles with an average diameter of ∼20 nm. The effect of the nitridation temperature and holding time on the powder properties is discussed.
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Li et al. (2001) studied this question.
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