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PLZT powder may be prepared by suspending PbO in a mixture of Zr(OBu)4 and Ti(OBu)4 by rapid stirring, and hydrolyzing the butoxides with an aqueous solution of La(Ac)3. Hydrolysis is completed and the PbO partially dissolved by addition of glacial acetic acid. The resulting suspension is dried, calcined, and rendered homogeneous by ball milling.
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Brooks et al. (1980) studied this question.
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