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The temperature dependence of the 1H second moment of the NMR line, the spin—lattice relaxation time, and the heat capacity in polycrystalline 1,3-cyclohexanedione is measured. The existence of the interesting isomorphous phase transition at 287 K is strongly confirmed. The stochastic ring conformational motion and large amplitude molecular rearrangement are characterised.
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Pająk et al. (1992) studied this question.
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