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Strontium hexaferrite (SrFe12O19) powder was synthesized by sol-gel based combustion technique. In this technique, strontium and iron nitrates were used as the source nitrates and D-fructose as the fuel. The phase formation, thermal properties, particle morphology and surface morphology of the sintered pellets were analyzed by X-ray diffraction (XRD), thermogravimetry/differential thermal analysis (TG-DTA) and high-resolution scanning electron microscope (HR-SEM). Crystalline particles obtained by the calcinations of the precursor powder at 900°C, showed the crystalline diffraction pattern with the corresponding major angles, 30.41°, 31.02°, 32.37°, 34.24°, 35.81°, 37.21°, 40.47° and 42.60° respectively. HR-SEM studies have revealed that the structure of calcined particles is a mixed hexagonal and nearly plate like hexagonal, and the surface of the sintered pellets results in hexagonal structure with good magnetic properties.
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Kanagesan et al. (2010) studied this question.
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