We used the piezoresponse mode of scanning force microscopy (SFM) to perform the first nanoscale observation of ferroelectric domain structure in as-grown SrBi2Ta2O9films. By lowering the loading force down to approximately 1 nN and by keeping the imaging voltage just below the coercive voltage, we managed to obtain a sufficiently high contrast between opposite 180° domains without affecting the original domain structure. Local and large-scale ferroelectric switching with subsequent readout in areas of about 0.01 µm2and 1.5 µm2, respectively, were carried out by applying pulsed- and dc-voltage bias through the conductive tip.
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Gruverman et al. (1998) studied this question.
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