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In this study, a transition metal‐free and thiol‐free method for constructing a series of highly functionalized thioesters has been developed, achieving moderate to good yields from benzothiazolium bromides, aroyl chlorides and H 2 O in a three‐component reaction, via an acid‐base‐promoted hydrolysis ring‐opening tandem reaction process. The present protocol features available starting materials, operational simplicity, and mild reaction conditions.
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Gao et al. (2026) studied this question.
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