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In situ surface-enhanced Raman scattering (SERS) was applied to observe the early stage of the formation of Ag nanoparticles in solution under microwave (MW) irradiation. Rise of SERS successfully observed for Rhodamine 6G confirmed homogeneous particle formation due to homogeneous and rapid heating under MW irradiation.
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Tsukahara et al. (2006) studied this question.
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